Hypothesis
Axion-like dark matter in the 10⁻²⁴ to 10⁻¹⁷ eV mass range would show up as an oscillating neutron electric dipole moment or an axion-wind spin-precession effect in stored ultracold neutrons and mercury-199 atoms.
What failed
Analysis of the ratio of neutron and ¹⁹⁹Hg spin-precession frequencies found no signal consistent with dark matter anywhere in that mass range.
Broken assumption
Ultralight axion dark matter couples to nucleons strongly enough to be seen in neutron EDM spin-precession data.
Why
No signal was present at the experiment's sensitivity; the null was turned into the first laboratory limits on axion-gluon coupling and tighter limits on axion-nucleon coupling.
From the published paper: Abel et al. Physical Review X, 2017. ↗CC BY